Structures by: Xiao W.

Total: 63

C30H27N3O5

C30H27N3O5

Xiao, WanlongMo, YuhaoGuo, JingSu, ZhishanDong, ShunxiFeng, Xiaoming

Chemical Science (2021)

a=10.8152(2)Å   b=12.5754(2)Å   c=20.1202(3)Å

α=90°   β=90°   γ=90°

C52H42N2O10,2(CDCl3)

C52H42N2O10,2(CDCl3)

Xiao, WanlongMo, YuhaoGuo, JingSu, ZhishanDong, ShunxiFeng, Xiaoming

Chemical Science (2021)

a=11.8889(4)Å   b=14.4911(5)Å   c=14.9954(5)Å

α=90°   β=104.794(2)°   γ=90°

C55H46Cl2N2O11

C55H46Cl2N2O11

Xiao, WanlongMo, YuhaoGuo, JingSu, ZhishanDong, ShunxiFeng, Xiaoming

Chemical Science (2021)

a=19.2448(5)Å   b=19.2448(5)Å   c=26.8461(8)Å

α=90°   β=90°   γ=90°

SrSiO3

O3SiSr

Xiao, W.Tan, D.Zhou, W.Liu, J.Xu, J.

American Mineralogist (2013) 98, 2096-2104

a=3.5034(7)Å   b=3.5034(7)Å   c=3.5034(7)Å

α=90°   β=90°   γ=90°

C12H13NO4

C12H13NO4

Xiao, WeiYin, XiangZhou, ZhiDu, WeiChen, Ying-Chun

Organic letters (2016) 18, 1 116-119

a=7.72422(10)Å   b=8.94615(12)Å   c=17.2197(2)Å

α=90°   β=101.0489(13)°   γ=90°

C16H14N2O2

C16H14N2O2

Yang, Qian-QianXiao, WeiDu, WeiOuyang, QinChen, Ying-Chun

Chemical communications (Cambridge, England) (2018) 54, 9 1129-1132

a=7.7601(3)Å   b=11.4659(4)Å   c=14.7078(5)Å

α=90°   β=90°   γ=90°

C41H34Cl3NO2PS

C41H34Cl3NO2PS

Hong-Gang ChengBin FengLi-Yan ChenWei GuoXiao-Ye YuLiang-Qiu LuJia-Rong ChenWen-Jing Xiao

Chem.Commun. (2014) 50, 2873

a=11.247(3)Å   b=17.258(4)Å   c=19.487(5)Å

α=90.00°   β=90.00°   γ=90.00°

C21H15N5O4,0.5(C4H8O2)

C21H15N5O4,0.5(C4H8O2)

Jinhu WeiWenbo XiaoCong-Ying ZhouChi-Ming Che

Chem.Commun. (2014) 50, 3373

a=8.0842(9)Å   b=12.2092(13)Å   c=12.7761(14)Å

α=73.1170(10)°   β=73.449(2)°   γ=79.959(2)°

{Cu6(tib)8(OH)4](OH)8.4CH3OH.22H2O

C37H54Cu1.5N12O9.5

Liu, Hong-KeTan, Hai-YanLiao, SenXiao, WenZhang, Hua-XinYu, Xiao-LanKang, Bei-ShengCai, Ji-WenZhou, Zhong-YuanChan, Albert S. C.

Chemical Communications (2001) 11 1008

a=13.662(2)Å   b=23.197(4)Å   c=18.914(4)Å

α=90.00°   β=110.074(3)°   γ=90.00°

C16H14F3N3O2

C16H14F3N3O2

Xing-Long YuJia-Rong ChenDong-Zhen ChenWen-Jing Xiao

Chem.Commun. (2016) 52, 8275

a=10.013(2)Å   b=7.5562(16)Å   c=21.159(5)Å

α=90°   β=93.102(3)°   γ=90°

C26H31NO5

C26H31NO5

Qiao-Hui DengJia-Rong ChenQiang WeiQuan-Qing ZhaoLiang-Qiu LuWen-Jing Xiao

Chem.Commun. (2015) 51, 3537

a=29.508(5)Å   b=8.3721(14)Å   c=19.678(3)Å

α=90°   β=90°   γ=90°

C26H24N4O2

C26H24N4O2

Xiao-Qiang HuJia-Rong ChenShuang GaoBin FengLiang-Qiu LuWen-Jing Xiao

Chem.Commun. (2013) 49, 7905

a=25.251(4)Å   b=11.0982(16)Å   c=18.647(3)Å

α=90.00°   β=122.073(2)°   γ=90.00°

C31H26N4O2

C31H26N4O2

Xiao-Qiang HuJia-Rong ChenShuang GaoBin FengLiang-Qiu LuWen-Jing Xiao

Chem.Commun. (2013) 49, 7905

a=10.667(3)Å   b=27.905(7)Å   c=9.770(2)Å

α=90.00°   β=96.429(5)°   γ=90.00°

C12H12N2O

C12H12N2O

Jing An Ning-Jie ChangLi-Dong SongYu-Qin JinYing MaJia-Rong Chen Wen-Jing Xiao

Chem.Commun. (2011) 47, 1869

a=10.5035(12)Å   b=8.0361(9)Å   c=12.2743(14)Å

α=90.00°   β=98.375(2)°   γ=90.00°

C15H17NO4S

C15H17NO4S

Shu-Wen DuanYang LiYi-Yin LiuYou-Quan ZouDe-Qing ShiWen-Jing Xiao

Chem.Commun. (2012) 48, 5160

a=9.6237(6)Å   b=11.9478(7)Å   c=12.4395(8)Å

α=90.00°   β=90.00°   γ=90.00°

C28H24ClNO2S

C28H24ClNO2S

Honggang ChengLiang-Qiu LuTao WangJia-Rong ChenWen-Jing Xiao

Chem.Commun. (2012) 48, 5596

a=12.290(4)Å   b=5.9017(17)Å   c=16.991(5)Å

α=90.00°   β=104.225(5)°   γ=90.00°

C29H28N2O2S

C29H28N2O2S

Jun XuanYing ChengJing AnLiang-Qiu LuXiao-Xiao Zhang'Wen-Jing Xiao

Chem.Commun. (2011) 47, 8337

a=7.9943(10)Å   b=16.668(2)Å   c=18.837(2)Å

α=90.00°   β=90.00°   γ=90.00°

C20H24N2O10

C20H24N2O10

Xiao, WeimingChen, ChaoDeng, ShengjunMao, XuejinSun, BinZhang, Ning

CrystEngComm (2010) 12, 7 2011

a=6.2017(9)Å   b=8.3441(13)Å   c=9.6508(14)Å

α=91.155(2)°   β=93.378(2)°   γ=94.221(2)°

C24H42N4O14

C24H42N4O14

Xiao, WeimingChen, ChaoDeng, ShengjunMao, XuejinSun, BinZhang, Ning

CrystEngComm (2010) 12, 7 2011

a=7.260(3)Å   b=12.744(6)Å   c=16.409(8)Å

α=75.833(7)°   β=88.378(7)°   γ=87.605(7)°

2-Ethoxy-3-isopropylbenzo[4,5]thieno[3,2-d]pyrimidin-4(3H)-one

C15H16N2O2S

Sheng-Zhen XuMin-Hui CaoYang-Gen HuMing-Wu DingWen-Jing Xiao

Acta Crystallographica Section E (2005) 61, 9 o2789-o2790

a=13.3930(16)Å   b=6.8922(8)Å   c=15.4970(18)Å

α=90.00°   β=90.00°   γ=90.00°

(1R,2R,2'S)-2-(4-Methylphenylsulfonamido)-1-(pyrrolidine-2'- carboxamido)cyclohexane

C18H27N3O3S

Xinyong LiJiarong ChenXianggao MengWenjing Xiao

Acta Crystallographica Section E (2005) 61, 8 o2730-o2732

a=9.8855(7)Å   b=9.8856(7)Å   c=20.3477(14)Å

α=90.00°   β=90.00°   γ=90.00°

1,1'-Diacetylferrocene bis(thiosemicarbazone) monohydrate

C16H22FeN6OS2

Wen XiaoZhong-Lin LuRui-Ying LiCheng-Xong SuBei-Sheng KangS. Shanmuga Sundara RajHoong-Kun Fun

Acta Crystallographica Section C (1999) 55, 11 1762-1764

a=29.0676(2)Å   b=8.80130(10)Å   c=18.44700(10)Å

α=90.00°   β=125.9780(10)°   γ=90.00°

C6H18N2O11S

C6H18N2O11S

Zhang, HongWang, Ximin Chang, Xienan Xiao, Weiqiang Zhang, Kecong Teo, Boon K.

Acta Crystallographica Section C (1997) 53, 9 1286-1288

a=10.597(2)Å   b=21.337(2)Å   c=5.8550(10)Å

α=90°   β=90°   γ=90°

P-Methoxybenzaldehyde Isonicotinoyl Hydrazone Monohydrate

C14H13N3O2,H2O

S.Shanmuga Sundara RajHoong-Kun FunZhong-Lin LuWen XiaoYe-Xiang TongBei-Sheng Kang

Acta Crystallographica Section C (1999) 55, 6 942-944

a=7.3875(2)Å   b=12.4718(3)Å   c=14.8382(4)Å

α=90.00°   β=96.7270(10)°   γ=90.00°

1,4-Bis(5,5-dimethyl-2-oxo-4-phenyl-1,3,2-dioxaphosphorinan-2-yl)piperazine

C26H36N2O6P2

Xuemei ChenWensheng XiaoPing Jiao

Acta Crystallographica Section E (2007) 63, 11 o4271-o4271

a=6.4436(7)Å   b=10.4563(11)Å   c=11.5762(13)Å

α=65.680(2)°   β=86.755(2)°   γ=72.641(2)°

P-Methoxybenzaldehyde Benzoylhydrazone Monohydrate

C15H14N2O2,H2O

Shanmuga Sundara Raj, S.Fun, Hoong-KunLu, Zhong-LinXiao, WenGong, Xiao-YangGen, Chang-Ming

Acta Crystallographica Section C (2000) 56, 8 1013-1014

a=11.9398(6)Å   b=11.8595(6)Å   c=11.3972(6)Å

α=90.00°   β=116.3890(10)°   γ=90.00°

3-Methoxy-4-hydroxyl-benzaldehyde 4,5-Diaza-9-fluorenylidenehydrazone

C19H14N4O2

Shanmuga Sundara Raj, S.Fun, Hoong-KunLu, Zhong-LinXiao, WenGong, Xiao-YangGen, Chang-Ming

Acta Crystallographica Section C (2000) 56, 8 1015-1016

a=7.5130(2)Å   b=26.9091(5)Å   c=7.91410(10)Å

α=90.00°   β=90.00°   γ=90.00°

4,5-Diaza-9-fluorenone Benzoylhydrazone Monohydrate

C18H12N4O,H2O

Lu, Zhong-LinXiao, WenChen, Zhong-NingGong, Xiao-YangShanmuga Sundara Raj, S.Razak, Ibrahim AbdulFun, Hoong-Kun

Acta Crystallographica Section C (2000) 56, 8 1017-1018

a=8.4880(2)Å   b=22.7523(2)Å   c=8.7810(2)Å

α=90.00°   β=114.9290(10)°   γ=90.00°

10-Hexyl-10<i>H</i>-phenothiazine-3-carbaldehyde

C19H21NOS

Wang, HongliXu, WenyuanZhang, BinXiao, WenjingWu, Hong

Acta Crystallographica Section E (2008) 64, 12 o2458

a=8.4073(9)Å   b=13.7719(15)Å   c=14.6485(15)Å

α=93.957(2)°   β=98.781(2)°   γ=90.983(2)°

4-(Diphenylamino)benzaldehyde

C19H15NO

Wang, HongliXu, WenyuanZhang, BinXiao, WenjingWu, Hong

Acta Crystallographica Section E (2009) 65, 1 o149

a=12.1188(8)Å   b=11.4342(8)Å   c=10.9560(7)Å

α=90.00°   β=102.082(2)°   γ=90.00°

N,N'-Di-(tert-butylsulfinyl)-1,2-di-tert-butylethane-1,2-diamine

C18H40N2O2S2

Sun, XiaoxiaHu, YuFan, CongbinXiao, Weihong

Acta Crystallographica Section E (2009) 65, 1 o172

a=13.053(2)Å   b=9.5780(10)Å   c=18.279(2)Å

α=90.00°   β=92.069(8)°   γ=90.00°

Tetrakis[(4-methoxycarbonyl)anilinium] hexachloridostannate(IV) dichloride

4(C8H10NO2),Cl6Sn2,2(Cl)

Xiao, WenzhiXue, RuitingYin, Yansheng

Acta Crystallographica Section E (2011) 67, 3 m297

a=30.748(3)Å   b=7.1172(8)Å   c=22.113(2)Å

α=90.00°   β=119.424(2)°   γ=90.00°

2-Aminobenzene-1,4-dicarboxylic acid--4,4'-bipyridine (1/1)

C18H15N3O4

Xiao, WenzhiXue, RuitingYin, Yansheng

Acta Crystallographica Section E (2011) 67, 6 o1333

a=16.9501(18)Å   b=11.1959(13)Å   c=9.2510(10)Å

α=90.00°   β=116.986(2)°   γ=90.00°

Chlorido{μ-2,6-bis[(2-aminoethyl)iminomethyl]-4-chlorophenolato}-μ-oxido- dicopper(II) trihydrate

C14H20Cl2Cu2N4O2,3(H2O)

Zhou, Jing-JingXiao, WeiMao, Jia-WeiZhou, Hong

Acta Crystallographica Section E (2012) 68, 6 m794-m795

a=11.201(5)Å   b=12.387(7)Å   c=16.718(7)Å

α=90.00°   β=93.18(4)°   γ=90.00°

(11a<i>S</i>)-7-Bromo-2,3,5,10,11,11a-hexahydro-1<i>H</i>- pyrrolo[2,1-<i>c</i>][1,4]benzodiazepine-3,11-dione

C12H11BrN2O2

Ma, ChaoWang, Zhen-ZhongPan, LiTian, YuXiao, Wei

Acta Crystallographica Section E (2012) 68, 1 o126

a=4.3880(4)Å   b=13.1210(11)Å   c=19.8722(16)Å

α=90.00°   β=90.00°   γ=90.00°

Bis[<i>N</i>-(2-furylmethyl)ethane-1,2-diamine]bis(perchlorato)copper (II)

C14H24Cl2CuN4O10

Xiao, WeiLi, Shi-RongZhou, HongPan, Zhi-QuanHuang, Qimao

Acta Crystallographica Section E (2011) 67, 6 m701

a=9.736(8)Å   b=11.899(9)Å   c=9.466(7)Å

α=90.00°   β=94.227(12)°   γ=90.00°

C32.6H30.55N2.78O16.81S4

C32.6H30.55N2.78O16.81S4

Xiao, WenchangHu, ChunhuaWard, Michael D.

Crystal Growth & Design (2013) 13, 7 3197

a=21.150(4)Å   b=18.254(3)Å   c=15.735(3)Å

α=90°   β=109.559(3)°   γ=90°

C18H26N8O9S2

C18H26N8O9S2

Xiao, WenchangHu, ChunhuaCarter, Damien J.Nichols, ShaneWard, Michael D.Raiteri, PaoloRohl, Andrew L.Kahr, Bart

Crystal Growth & Design (2014) 14, 8 4166

a=6.8426(5)Å   b=20.0479(14)Å   c=21.4663(15)Å

α=90.00°   β=90.00°   γ=90.00°

C24H28N6O6S2

C24H28N6O6S2

Adachi, TakujiConnors, David M.Xiao, WenchangHu, ChunhuaWard, Michael D.

Crystal Growth & Design (2015) 15, 7 3366

a=19.603(3)Å   b=7.6017(10)Å   c=19.639(3)Å

α=90°   β=112.7510(17)°   γ=90°

C30H32N6O6S2

C30H32N6O6S2

Adachi, TakujiConnors, David M.Xiao, WenchangHu, ChunhuaWard, Michael D.

Crystal Growth & Design (2015) 15, 7 3366

a=21.1455(19)Å   b=12.7188(12)Å   c=17.8085(16)Å

α=90°   β=105.0780(16)°   γ=90°

C24H28N6O6S2

C24H28N6O6S2

Adachi, TakujiConnors, David M.Xiao, WenchangHu, ChunhuaWard, Michael D.

Crystal Growth & Design (2015) 15, 7 3366

a=21.7900(10)Å   b=7.5850(3)Å   c=16.3519(7)Å

α=90°   β=90°   γ=90°

C24H20O6

C24H20O6

Zhang, JianlinLiu, XiaohuaGuo, SongsongHe, ChangqiangXiao, WanlongLin, LiliFeng, Xiaoming

The Journal of organic chemistry (2018) 83, 17 10175-10185

a=10.8962(4)Å   b=16.0389(4)Å   c=11.6123(3)Å

α=90°   β=104.434(3)°   γ=90°

2(C34H32O6)

2(C34H32O6)

Zhang, JianlinLiu, XiaohuaGuo, SongsongHe, ChangqiangXiao, WanlongLin, LiliFeng, Xiaoming

The Journal of organic chemistry (2018) 83, 17 10175-10185

a=10.7835(3)Å   b=24.3459(5)Å   c=11.8380(3)Å

α=90°   β=115.986(4)°   γ=90°

C7.5H7.5F7.5N7.5O7.5S0.75

C7.5H7.5F7.5N7.5O7.5S0.75

Wang, WeilinCao, XiaohuiXiao, WeiguoShi, XiaoyuZuo, XiaodanLiu, LingyanChang, WeixingLi, Jing

The Journal of organic chemistry (2020)

a=15.825(3)Å   b=7.3310(15)Å   c=18.791(4)Å

α=90°   β=102.94(3)°   γ=90°

C19H15BrO4

C19H15BrO4

Ying ChengJing AnLiang-Qiu LuLan LuoZheng-Yi WangJia-Rong ChenWen-Jing Xiao

Journal of Organic Chemistry (2011) 76, 281-284

a=5.6153(8)Å   b=16.599(2)Å   c=18.194(2)Å

α=90.00°   β=90.00°   γ=90.00°

C16H12BrNO3

C16H12BrNO3

Liang-Qiu LuZhi-Hui MingJing AnChao LiJia-Rong ChenWen-Jing Xiao

Journal of Organic Chemistry (2012) 77, 1072-1080

a=7.9944(11)Å   b=6.2207(9)Å   c=14.801(2)Å

α=90.00°   β=103.384(2)°   γ=90.00°

C22H18O2S

C22H18O2S

Hong CaoWen-Jing XiaoHoward Alper

Journal of Organic Chemistry (2007) 72, 8562-8564

a=5.7476(16)Å   b=10.267(3)Å   c=29.264(8)Å

α=90.00°   β=90.00°   γ=90.00°

C33H29NO9W

C33H29NO9W

Jinzhu ChenZhengkun YuZhaoyan ZhengKaichun GuSizhong WuFanlong ZengWeiqiang TanXiaowei WuWenjing Xiao

Organometallics (2005) 24, 302-308

a=11.1571(9)Å   b=13.6990(11)Å   c=11.3873(10)Å

α=90.00°   β=113.103(2)°   γ=90.00°

C38H29Cr2NO13

C38H29Cr2NO13

Jinzhu ChenZhengkun YuZhaoyan ZhengKaichun GuSizhong WuFanlong ZengWeiqiang TanXiaowei WuWenjing Xiao

Organometallics (2005) 24, 302-308

a=12.5659(9)Å   b=20.5264(14)Å   c=14.4656(10)Å

α=90.00°   β=90.1920(10)°   γ=90.00°

C20H15NO7W

C20H15NO7W

Jinzhu ChenZhengkun YuZhaoyan ZhengKaichun GuSizhong WuFanlong ZengWeiqiang TanXiaowei WuWenjing Xiao

Organometallics (2005) 24, 302-308

a=7.4353(7)Å   b=12.1255(11)Å   c=12.5732(12)Å

α=65.069(2)°   β=82.996(2)°   γ=79.906(2)°

C28H29NO5

C28H29NO5

Jinzhu ChenZhengkun YuZhaoyan ZhengKaichun GuSizhong WuFanlong ZengWeiqiang TanXiaowei WuWenjing Xiao

Organometallics (2005) 24, 302-308

a=38.242(9)Å   b=7.1774(17)Å   c=17.705(4)Å

α=90.00°   β=92.733(5)°   γ=90.00°

C16H13NO3

C16H13NO3

Liang-Qiu LuYi-Ju CaoXiao-Peng LiuJing AnChang-Jiang YaoZhi-Hui MingWen-Jing Xiao

Journal of the American Chemical Society (2008) 130, 6946-6948

a=7.8191(5)Å   b=26.6567(13)Å   c=6.3613(7)Å

α=90.00°   β=98.6590(10)°   γ=90.00°

C30H18O12S4,3(C7H8),C4H8O2,4(CH6N3)

C30H18O12S4,3(C7H8),C4H8O2,4(CH6N3)

Xiao, WenchangHu, ChunhuaWard, Michael D.

Journal of the American Chemical Society (2014) 136, 40 14200

a=6.1781(11)Å   b=35.439(6)Å   c=15.264(3)Å

α=90.00°   β=100.518(3)°   γ=90.00°

C50H74N12O20S4

C50H74N12O20S4

Xiao, WenchangHu, ChunhuaWard, Michael D.

Journal of the American Chemical Society (2014) 136, 40 14200

a=6.001(3)Å   b=35.559(15)Å   c=15.223(6)Å

α=90.00°   β=101.047(4)°   γ=90.00°

C54H82.18N12O22.17S4

C54H82.18N12O22.17S4

Xiao, WenchangHu, ChunhuaWard, Michael D.

Journal of the American Chemical Society (2014) 136, 40 14200

a=16.049(4)Å   b=18.303(4)Å   c=35.233(8)Å

α=80.303(3)°   β=85.430(3)°   γ=77.818(3)°

C54H82.18N12O22.17S4

C54H82.18N12O22.17S4

Xiao, WenchangHu, ChunhuaWard, Michael D.

Journal of the American Chemical Society (2014) 136, 40 14200

a=16.068(4)Å   b=18.326(4)Å   c=35.252(8)Å

α=80.336(3)°   β=85.481(3)°   γ=77.775(3)°

C54H82N12O17S4

C54H82N12O17S4

Xiao, WenchangHu, ChunhuaWard, Michael D.

Journal of the American Chemical Society (2014) 136, 40 14200

a=12.043(5)Å   b=15.891(6)Å   c=34.087(13)Å

α=84.671(5)°   β=87.393(5)°   γ=83.725(4)°

C18H48N18O18S6

C18H48N18O18S6

Liu, YuzhouXiao, WenchangYi, Jin JuHu, ChunhuaPark, Sang-JaeWard, Michael D.

Journal of the American Chemical Society (2015) 137, 9 3386-3392

a=10.013(2)Å   b=21.303(4)Å   c=10.071(2)Å

α=90.00°   β=103.21(3)°   γ=90.00°

C14H34N12O12S4

C14H34N12O12S4

Liu, YuzhouXiao, WenchangYi, Jin JuHu, ChunhuaPark, Sang-JaeWard, Michael D.

Journal of the American Chemical Society (2015) 137, 9 3386-3392

a=7.4352(2)Å   b=9.8700(3)Å   c=10.2119(3)Å

α=74.4080(10)°   β=82.6280(10)°   γ=87.0200(10)°

C40H54N12O14S4

C40H54N12O14S4

Liu, YuzhouXiao, WenchangYi, Jin JuHu, ChunhuaPark, Sang-JaeWard, Michael D.

Journal of the American Chemical Society (2015) 137, 9 3386-3392

a=7.3536(14)Å   b=12.290(2)Å   c=17.228(3)Å

α=98.787(2)°   β=92.441(2)°   γ=94.135(2)°

C24H32Cd4N8O8S8

C24H32Cd4N8O8S8

Hong ZhangXimin WangH. ZhuW. XiaoKecong ZhangBoon K. Teo

Inorganic Chemistry (1999) 38, 886-892

a=11.604(7)Å   b=11.366(7)Å   c=15.736(4)Å

α=90°   β=92.84(3)°   γ=90°

C22H32Cd3N6O8S6

C22H32Cd3N6O8S6

Hong ZhangXimin WangH. ZhuW. XiaoKecong ZhangBoon K. Teo

Inorganic Chemistry (1999) 38, 886-892

a=16.297(3)Å   b=26.267(3)Å   c=16.296(2)Å

α=90°   β=90.20(1)°   γ=90°

1,4-diazoniabicyclo[2.2.2]octane 3,3'-dicarboxy-biphenyl-4,4'-dicarboxylate dihydrate

C22H26N2O10

Weiming XiaoChao ChenBin SunNing Zhang

Zeitschrift für Kristallographie - New Crystal Structures (2012) 227, 2 151

a=6.5808(12)Å   b=12.609(3)Å   c=12.765(2)Å

α=81.731(3)°   β=85.688(3)°   γ=87.024(3)°